1-(4-Formyl-2,6-dimethoxyphenoxy)-4-chlorobut-2-yne
Affiliation auteurs | Affiliation ok |
Titre | 1-(4-Formyl-2,6-dimethoxyphenoxy)-4-chlorobut-2-yne |
Type de publication | Journal Article |
Year of Publication | 2021 |
Auteurs | Husson J |
Journal | MOLBANK |
Volume | 2021 |
Pagination | M1252 |
Date Published | SEP |
Type of Article | Article |
Mots-clés | alkyne derivatives, ether derivatives, O-alkylation, Williamson reaction |
Résumé | A reaction of biomass-derived aldehyde synringaldehyde and half an equivalent of 1,4-dichlorobut-2-yne was attempted in order to obtain a bis-aldehyde with an alkyne spacer. The reaction was carried out in a basic media to effect bis O-alkylation, as described in literature for the preparation of structurally similar compounds. Nevertheless, only mono alkylation was observed. |
DOI | 10.3390/M1252 |